Complete validation support for GLP GMP practice

The AUT-701 Titrator can track users with access permissions, and track electrode calibration, serial number, date, time, operator, etc. Our patented electrode memory sotres all the calibration data and serial number with the electrode. When a sensor is changed, the data is automatically downloaded to the instrument. Data can be tracked, stored and printed or sent to a host computer for logging.

Complete validation and automation is possible with the software package available with the AUT-701. Both an onboard printer and external printer is available. LAN/ethernet as well as USB ports built in.

Features:

• User name and password access rights with administrative rights. Logged for each titration
• Ambient temperature and Relative humidiy can be logged (option)
• Electrode memory allows for complete calibration history for each sensor connected.
• Methods and other information can be stored and loaded from a USB memory drive.
• Software allows for real time data acqusition and instrument memory archive.

Single, Multiple, and Dynamically linked Titration Methods and Routines:

There are many types of titration methods which can be performed. Methods include "Full Auto" for automatic end point detection and "End Level" for pre-set end-point level titrations. pH Stat titrations can be performed, and the system allows for complete control and automation of Conductivity ("V" and "L" type intersection) Methods. Special Algorythms for Petroleum Neutralization Titrations are also built-in. Also a few special routines are built in for Acidity, Salinity, Alkali, and Total Hardness.

The Control parameters are fully programmable and extremely flexible to accomodate the most demanding titration requirements. Full calculation control for up to 5 end points, linking of multiple titrations using multiple pre-amps is possible. Amperometric and colorimetric analysis is simple with the available sealed titration cell, photometric adapter and wide range on electrode systems.

Micro-titrations are now possible with the small volume titration adapter.

With the sampling device, you can completely automate your procedure from running the calibration standards, then standardizing the titrant, and then automatically running multiple samples without any operator intervention.

AUT-701 Titration Methods

The AUT-701 has the ability to perform many types of titration methods. This allows for unmatched flexibility to perform all type of titrations. A true recalculation mode allows for re-analysis of previous data after control parameters or calculation formulas have been modified.

Listed below are the methods available as standard equipment on the AUT-701. Also identified are a few important control parameters and explanation as to how they work.

Method Number	Type of Method	Description
1 (201)	Neutralization Titration	Automatic infelction detection Standard Mode for titration using automatic detection by 1st derivative. (Max potential change/volume increment). (up to 5 EP's w/calculations)
2 (202)	Neutralization Titration by Set Point	Standard Mode for Set point titration. (Volume at preset ph or mv level(s)), 2 set points
3 (203)	Full volume Titration Auto EP detection after Max. Volume/potential reached.	Used to titrate to a fixed volume or potential and then analyze data for end points based on programmable control parameters(ncluding Auto or set points). Extremely flexible and important when using the re-calculation mode. All data is resident.
4 (204)	Blank Titration Mode	Used to measure very small volumes in blank titration
5 (205)	Non-Aqueous Titration Mode	Used for Non-aqueous titrations. Uses very good potential stability parameters for equilibrium between additions.
6 (206)	Potentiometric Titration small potential change at inflection	Used primarily for precipitation, red-ox, or chelate titrations with ion electrode with a small potential change at the end point.
7 (207)	Potentiometric Titration large potential change at inflection	Used primarily for titrations with a large potential change at the end point. (strong acid / strong base titration)
8 (208)	Conductivity Titration, Mode 1	Unique conductometric titration. EP is determined by "V" intersection. EP is judged as the point of intersection of two lines after titration.
9 (209)	Conductivity Titration, Mode 2	Unique conductometric titration. EP is determined by "L" intersection. EP is judged as the point of intersection of two lines after titration.
10 (210)	Petroleum Neutralization Titration, Mode 1	Total Base value of petroleum (TBN), Hydrochloric, non-aqueous titration. (ASTM 664)
11 (211)	Petroleum Neutralization Titration, Mode 2	Total Acid value of petroleum (TAN), Perchloric, non-aqueous titration. (ASTM 2896)
12 (2123)	Petroleum Neutralization Titration, Mode 3	Mode for measuring strong acid value + total acid value, strong base value + total base value
13 (213)	pH Stat titration, pH adjustment, Mode 1	Standard mode for pH stat analysis for unknown buffering action in sample.
14 (214)	pH Stat titration, pH adjustment, Mode 2	pH stat analysis for strong buffering action in sample.
15 (215)	pH Stat titration, pH adjustment, Mode 3	pH stat analysis for weak buffering action in sample.
16 (216)	Acidity Titration Mode	Dedicated for measuring Acidity
17 (217)	Salinity Titration Mode	Dedicated for measuring Salinity
18 (218)	Alkalinity Titration Mode	Dedicated for measuring Alkalinity
19 (219)	Total hardness Titration Mode	Dedicated for measuring Total Hardness (Ca and Mg)
20 (220)	Preliminary Test Titration Mode	Used to help the operator determine the best titration parameters upon initial titration of a new sample. This mode uses the automatic EP detection algorythm. 21 to 60 User Methods Mode Used to custom tailor titration methods specific to the customers application. Freely programmable and can incorporate all of the parameters of the standard pre-defined methods. Ful calculation control is possible. Parameters also include titrating buret (1-10), electrode preamp and type, etc.
111 to 130	Link Mode	Used to link other titration modes together to perform sequetial analysis of very complex titrations for one particular sample. Allows for multiple chemistries, dosing, and using all type of titration modes, reagents and electrode systems.
61 to 70	ABT Dispense Mode	Used to control the ABT-7 buret for adding a fixed volume of reagent. fully programmable rate, buret, etc.
71 to 80	AST Unit control Modes	Used for the AST measuring equipment
81 to 85	ABT Fixed Speed Injector	Used to control the ABT-7 buret for fixed speed injection of reagent. (buret 1-10, volume and speed)
86 to 89	pH Calibration Mode Used with the TTT-510 Sampler to automatically perform a 3 point pH calibration. 90-93 Potential Measurement Mode	Used to Measure potentials from attached preamps. Will be printed out. Select Electrode channel, preamp, wait time, etc.
94-100	Conc. Calculation Mode	Used for calculating the concentration using measured values from any other mode.
101-110	Divergence Mode	Used with the link mode, sets the destination to link based on the measured result
131-140	Reagent Checking	Test the titrator system by using standard reagents for periodic maintenance

Titration results from the AUT-701 Titrator

To the left is a typical printout which can be obtained with the AUT-701 Titrator. Notice the analog (or s-shaped) curve as well as the first derivative at the end point.

Up to 6 different print formats are available:

• Initial Info - EP Potential, Temp., titration Volume
• Time and titration volume -
• Time, potential, temerature -
• Time, Potential, temp, volume -
• Time, Volume -
• Time, potential, temp., volume -

Complete documentation is available via the onboard printer / plotter as well as external output to a LIMS system. There is also software available to output the data results to a PC for use with standard spreadsheet software for further data storage and recall or archiving purposes.

For more information, inquire about our AUT-LOG software control package.

For GLP/GMP Compliance, both real time and post titration or smoothed data can be obtained for record keeping. Notice the maximum first derivative value which corresponds to the end point of the titration. Also the electrode calibration date, time and information can be printed out.

Specifications: AUT-701 Main Unit

Measuring Range	pH: pH0.00 - 14.00, mV:0 to +/-1999.9mV, Temp: 0 to 100.0 C. Current/voltage: 0 - 2, 20, 200, 1000uA (by range Selection)/0.0-+/-2,000.0mv Conductivity: 7 ranges, 0.0 - 200.0 S/m (by range selection) % transmittence: 0.0 - 100.0% Ambient temp.; 0.0-50.0C Relative Humidity; 5-90%
pH Calibration	Automatic 3 point calibration (pH 4.01, 6.86, 9.18), Manual with other standards
Titration Method/Measuring Method	utomatic Inflection End point detection (Up to 5 points detectable) Set Point Titration (Up to 5 points detectable) Full Volume Titration (Inflection point plus set point) (Up to 5 points detectable) Intersection of two lines detection titration (Up to 2 points detectable) Stat Titration Preliminary titration(Automatic parameter evaluation method) pKa Measurement pH (mV) Measurement pH Adjustment Electric Conductivity measurement
Display	Color graphic LCD with Back light Titration Curve, Titration Volume, pH(mV), Temperature simultaneously displayed.
Keyboard Operation	Flat Keypad/ Dialogue operation system by function keys and numeric keypad.
Printer	Provided (Internal) thermal Printer. External dot matrix Printer is optional
Output	pH: +/-700mV (pH 0-14), mV: +/-1V, (0 to +/-1,999mV)
Number of electrode Input channels	Maximum of three channels 2 Channels of pH/mV electrode inputs are installed as standard. Third Channel can be installed as option: FUT-7050 Potentiometric unit FUT-7010 Photometric unit FUT-7030 Polarization unit FUT-7040 Conductivity unit
External Control I/O	RS-232C x 5 Channel 1CH: Automatic Buret (ABT-7 Connectable up to 10 units) 2CH: Personal Computer 3CH: Turn Table (TTT-510) 4CH: 1 from Electric Balance Interface, AST-3210 sampler, or TTT-510 5CH: External Printer, EPS-R LAN x 1 USB(Host) x 1
GLP applicable functions	Electrode Calibration Resume function Electrode replacement time notification
Power Requirements	AC Line 50, 60Hz
Power Consumption	50VA When Connecting one ABT-7 automatic Buret)
Dimensions	approx: 190(w)x192(h)x385(d)mm

Specifications: ABT-7 Automatic Buret

Indication	LED syringe size indication
Syringe size setting	Rotary switch
Syringe	Fine polished hard glass, 20 ml std. 20 ml brown glass syringe (1ml, 5ml, 10ml, 50ml option)
Wetted parts material	Hard glass, Teflon, Diflon
Tubing	2(ID) x 3(OD)mm Black Teflon Tube. (1(ID) x 3(OD) for 1ml syringe)
Absorption Speed	Approx. 20 Seconds full stroke.,/font>
Dispensing Speed/ Minimum titration volume	50 ml syringe: 2 - 150 ml/min / 0.0025ml 20 ml syringe: 0.6 - 60 ml/min / 0.001ml 10 ml syringe: 0.3 - 30 ml/min / 0.0005ml 5 ml syringe: 0.2 - 15 ml/min / 0.00025ml 1 ml syringe: 0.03 - 3 ml/min / 0.00005ml
Buret Accuracy	Whole capacity error allowance: +/- 0.1%, Reproducability: +/- 0.01ml(at 20 ml syringe)
Validation support	Burette volume checking history: max 6
Outlet for peripherals	one for burette, one for mag. stirrer
Ambient Temp and RH	5-35C, 85% or less
Power Requirements	AC 100V-240V Line 50/60Hz
Power Consumption	approx. 30VA
Dimensions	approx: 110(w)x396(h)x346(d)mm

Standard Accessories: (AUT-701 Main)

1	GST-5741C	Strong pH Electrode
1	143F192	pH 6.86 Standard Buffer Solution (500 mls)
1	143F191	pH 4.01 Standard Buffer Solution (500 mls)
1	RE-4-05	Saturated KCL solution, 50 ml
1	OIB00001	Electrode Holder
1	6948810K	Electrode Stand with stop
1	ST-7	Magnetic Stirrer (110v or Specify Voltage)
1	OIB00004	Electrode attachment (G-type)
1	OIB00005	Electrode attachment (J-type)
1	PAP-HCSOIB00001	Thermal Printer Paper (Pack of 2 rolls)
1	Manual	Operation Manual

Standard Accessories: (ABT-7 Burette)

1	7075610K	Buret unit plate (for 1-20ml syringe)
1	AUT-045P	20 ml Brown glass syringe
1	AUT-066P	Metal Plunger puller tool
1	P000070	Brown Glass degassing nozzle for 1-20 ml syringe
1	AUT-067P	Nozzle cleaning wire
1	7075640K	CO2 adsorbent Soda Lime tube
1	7075630K	1000ml reagent bottle, translucent/ brown
1	AUT-022P	Teflon Tube, 2m
1	P000108	Tube for nozzle purge
1	118B641	Burette Connection cable, 0.9m
1	HEX-ACL3	Power Cord
1	Manual	Operation Manual